1. I am glad I discored this site:). They helped me, Introduction and preparation of salicylic acid (1), 21.2 - Part 2 Reactions of Carboxylic Acid Derivatives - Wade 7th, No public clipboards found for this slide. The experiment was carried out using a reflux condenser under heat because heat is needed to increase the rate of the reaction and the reflux … Vacuum filtered and measured the melting range of dry product. In the lab, it was apparent that all the students were able to use the air condenser and all other glassware used in the experiment. Fantastic that ⇒⇒⇒ ESSAYHELPONLINE.NET ⇐⇐⇐ can deliver my paper in just 3 hours when Im burning with my timeline.

The boiling point of methanol is 64.6 °C, so point the mouth of the tube away from others and avoid overheating, We use your LinkedIn profile and activity data to personalize ads and to show you more relevant ads.

This was due majorly for the fact that the filteration system on many of the suction faucets did not work, making for repeated trials while losing parts of product in the process. Heated reaction for 30 minutes after boiling started. Measured 2 mmol of methyl salicylate into conical vial.

Principle: Methyl salicylate (oil of wintergreen) is an organic ester. As of this date, Scribd will manage your SlideShare account and any content you may have on SlideShare, and Scribd's General Terms of Use and Privacy Policy will apply.

Theoretical Yield of Salicylic Acid (SA) (g): (.002038 mol Methyl Salicylate)*(1 mol SA/1 mol Methyl Salicylate)*(138.1 g SA/1 mol SA)= .281 g Salicylic Acid, (.002038 mol Methyl Salicylate)*(1 mol SA/1 mol Methyl Salicylate)*(138.1 g SA/1 mol SA)= .281 g Salicylic Scribd will begin operating the SlideShare business on December 1, 2020 Oil of Wintergreen: Synthesis and NMR Analysis O Introduction: When salicylic acid reacts with methanol in the presence of an acid catalyst, methyl salicylate, or oil of wintergreen, is produced according to the following equation: C OH OH + CH 3 OH H+ C OCH 3 O OH + H 2 O salicylic acid methanol methyl salicylate (oil of wintergreen) Measured 2 mmol of methyl salicylate into conical vial. Attached an air condenser to a conical vial. Chem213 section: 001 If you wish to opt out, please close your SlideShare account. <>/XObject<>/ProcSet[/PDF/Text/ImageB/ImageC/ImageI] >>/MediaBox[ 0 0 612 792] /Contents 4 0 R/Group<>/Tabs/S/StructParents 0>> Synthetic FFR 3. Support will always contact you if there is any confusion with the requirements of your paper so they can make sure you are getting exactly what you need. 3 0 obj <>>> One change that should be made to this lab is to proportion everything in higher quantities, making it easier to get certain quantities of liquid and transfer it with the accurate amount present. Add 2 drops of concentrated sulfuric acid.

Removed condenser when it was cool enough to touch, then waited till room temp. Purpose: Learn more. It is artificially synthesized to produce perfumes and fragrances, foods and beverages, and liniments. Slideshare uses cookies to improve functionality and performance, and to provide you with relevant advertising. Transferred the mixture to a beaker, then slowly added H 2 SO 4 until pH=2. This reaction is also termed as an esterification, since the product of the reaction is an ester, a compound co… See our User Agreement and Privacy Policy. %PDF-1.5 My melting point for the recrystallized salicylic acid was in a range of 125-130ᵒC, which did not overlap the literature value of 159ᵒF. Clipping is a handy way to collect important slides you want to go back to later.

4 0 obj Let mixture settle and then vacuum filtered the mixture. Synthesis of Methyl Salicylate via Amine Salicylic acid, prepared from the hydrolysis of methylsalicylate is reacted with acetic anhydride producing the ester product, acetylsalicylic acid. stream x��ZY��8~������[-��5; �dvz��fz�2��ږ�ڵEGG����*��(�jo��Y,���o_VM��V ��ۗM�����}�}P��n����SQfM�ʟf�^߱WW/n�,�҈=l�^p���B�{��2f��>{‡�_���`˿��oW/��R����ul�J5����Lw��$��F���Ż�M����M ������,o��}X�E�?˛t�/�� Now customize the name of a clipboard to store your clips. The prices are not expensive compared to other sites.

Turned off burner when mixture was clear. The type of reaction may be known as condensation reaction because the small molecule of H2O is eliminated from the reactants while the remaining bits of the reactants condense together to give the main product. Michael Banales Melting Point of the recrystallized salicylic acid: 125-130ᵒC. I have been using it since last year. Kaitlin Saloky Purpose The purpose of this lab was to convert acetylsalicylic acid to methyl salicylate while monitoring the reaction progress using TLC. Rashid Alsuwaidi In a previous experiment, we have used the Fischer esterification reaction to produce isopentyl acetate from an acid (acetic acid) and an alcohol (isopentyl alcohol).

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During recrystallization and analysis, the students learned how to locate and utilize solubility data and also determine melting points. Heated reaction for 30 minutes after boiling started. ⇒⇒⇒WRITE-MY-PAPER.net ⇐⇐⇐ I love this site. Place 0.5 g of salicylic acid and 3 mL of methanol in a large test tube. Synthesis of Salicylic Acid from Wintergreen Oil Synthesis of Salicylic Acid from Wintergreen Oil. endobj endobj Then cooled the solution to room temp, then cooled in ice bath for 8 minutes. �h��vf.��Z0e�Q��C���'�ĹJHOF�*�"%5�D��J���E �& �M�_���+�kO$����(bV��b���#[ �Ґ Z����-�������i��|�b�u��@"����%��t��w���?r5������~�j�,ߌF+���Xxql��ׇ7��/o���7��&:/��'��f�L|p��WE�C%1J�x_��,o�U>��%�N�WO~���+�([X�}|_��V�?��.�#/��т?�C�轷���E��.>Br/��I��mM��al����,���;Dr. Sometimes it feels like our professor wants to make us professors too by assigning so hard tasks so often and with a minimal interval for their finishing.


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